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Metal-Free Synthesis of 1,3-Disiloxanediols and Aryl Siloxanols
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https://doi.org/10.1021/acsomega.9b00121Abstract
The first example of metal-free oxidative hydrolysis of hydrido-siloxanes is reported. Both base-catalyzed and organocatalytic hydrolysis methods are demonstrated to transform 1,3-dihydrido-disiloxanes into 1,3-disiloxanediols. The first example of a chemoselective silane hydrolysis is demonstrated.
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